| For . . .
| You must . . .
| Using . . .
| According to the following requirements . . .
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| 1. Each lime kiln and each associated lime cooler, if there is a separate exhaust to the atmosphere from the associated lime cooler | Select the location of the sampling ports and the number of traverse points | Method 1 or 1A of appendix A-1 to 40 CFR part 60; and § 63.6(d)(1)(i) | Sampling sites must be located at the outlet of the control device(s) and prior to any releases to the atmosphere.
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| 2. Each lime kiln and each associated lime cooler, if there is a separate exhaust to the atmosphere from the associated lime cooler | Determine velocity and volumetric flow rate | Method 2, 2A, 2C, 2D, 2F, or 2G in appendices A-1 and A-2 to 40 CFR part 60 | Not applicable.
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| 3. Each lime kiln and each associated lime cooler, if there is a separate exhaust to the atmosphere from the associated lime cooler | Conduct gas molecular weight analysis | Method 3, 3A, or 3B in appendix A-2 to 40 CFR part 60 | You may use manual procedures (but not instrumental procedures) of ASME PTC 19.10-1981—Part 10 (see § 63.14 for availability) as an alternative to using Method 3B.
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| 4. Each lime kiln and each associated lime cooler, if there is a separate exhaust to the atmosphere from the associated lime cooler | Measure moisture content of the stack gas | Method 4 in appendix A-3 to 40 CFR part 60 | Not applicable.
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| 5. Each lime kiln and each associated lime cooler, if there is a separate exhaust to the atmosphere from the associated lime cooler, and which uses a negative pressure PM control device | Measure PM emissions | Method 5 in appendix A-3 to 40 CFR part 60 | Conduct the test(s) when the source is operating at representative operating conditions in accordance with § 63.7(e) before the relevant compliance date for your source as specified in §§ 63.7083(e) and 63.7112(b) on and after the relevant compliance date for your source as specified in § 63.7083(e); the minimum sampling volume must be 0.85 dry standard cubic meter (dscm) (30 dry standard cubic foot (dscf)); if there is a separate lime cooler exhaust to the atmosphere, you must conduct the Method 5 test of the cooler exhaust concurrently with the kiln exhaust test.
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| 6. Each lime kiln and each associated lime cooler, if there is a separate exhaust to the atmosphere from the associated lime cooler, and which uses a positive pressure FF or ESP | Measure PM emissions | Method 5D in appendix A-3 to 40 CFR part 60 | Conduct the test(s) when the source is operating at representative operating conditions in accordance with § 63.7(e) before the relevant compliance date for your source as specified in §§ 63.7083(e) and 63.7112(b) on and after the relevant compliance date for your source as specified in § 63.7083(e); If there is a separate lime cooler exhaust to the atmosphere, you must conduct the Method 5 or 5D test of the separate cooler exhaust concurrently with the kiln exhaust test. Refer to item 5 of this table for sampling time and volume requirements.
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| 7. Each lime kiln | Determine the mass rate of stone feed to the kiln during the kiln performance test | Any suitable device | Calibrate and maintain the device according to manufacturer's instructions; the measuring device used must be accurate to within ±5 percent of the mass rate of stone feed over its operating range.
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| 8. Each lime kiln equipped with a wet scrubber | Establish the operating limit for the average gas stream pressure drop across the wet scrubber during the PM and HCl performance test(s) | Data for the gas stream pressure drop measurement device during the kiln performance test | The continuous pressure drop measurement device must be accurate within plus or minus 1 percent; you must collect the pressure drop data during the period of the performance test and determine the operating limit according to § 63.7112(j).
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| 9. Each lime kiln equipped with a wet scrubber | Establish the operating limit for the average liquid flow rate to the scrubber during the PM and HCl performance test(s) | Data from the liquid flow rate measurement device during the kiln performance test | The continuous scrubbing liquid flow rate measuring device must be accurate within plus or minus 1 percent; you must collect the flow rate data during the period of the performance test and determine the operating limit according to § 63.7112(j).
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| 10. Each lime kiln equipped with a FF or ESP that is monitored with a PM detector | Have installed and have operating the BLDS or PM detector prior to the PM performance test | Standard operating procedures incorporated into the OM&M plan | According to the requirements in § 63.7113(d) or (e), respectively.
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| 11. Each lime kiln equipped with a FF or ESP that is monitored with a COMS | Have installed and have operating the COMS prior to the performance test | Standard operating procedures incorporated into the OM&M plan and as required by the general provisions of subpart A of this part and according to PS-1 of appendix B to 40 CFR part 60, except as specified in § 63.7113(g)(2) | According to the requirements in § 63.7113(g).
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| 12. Each stack emission from a PSH operation, vent from a building enclosing a PSH operation, or set of multiple storage bins with combined stack emissions, which is subject to a PM emission limit | Measure PM emissions | Method 5 or Method 17 in appendices A-3 and A-6 to 40 CFR part 60 | The sample volume must be at least 1.70 dscm (60 dscf); for Method 5, if the gas stream being sampled is at ambient temperature, the sampling probe and filter may be operated without heaters; and if the gas stream is above ambient temperature, the sampling probe and filter may be operated at a temperature high enough, but no higher than 121 °C (250 °F), to prevent water condensation on the filter (Method 17 may be used only with exhaust gas temperatures of not more than 250 °F).
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| 13. Each stack emission from a PSH operation, vent from a building enclosing a PSH operation, or set of multiple storage bins with combined stack emissions, which is subject to an opacity limit | Conduct opacity observations | Method 9 in appendix A-4 to 40 CFR part 60 | The test duration must be for at least 3 hours and you must obtain at least thirty, 6-minute averages.
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| 14. Each stack emissions source from a PSH operation subject to a PM or opacity limit, which uses a wet scrubber | Establish the average gas stream pressure drop across the wet scrubber during the PM and HCl performance test(s) | Data for the gas stream pressure drop measurement device during the PSH operation stack performance test | The pressure drop measurement device must be accurate within plus or minus 1 percent; you must collect the pressure drop data during the period of the performance test and determine the operating limit according to § 63.7112(j).
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| 15. Each stack emissions source from a PSH operation subject to a PM or opacity limit, which uses a wet scrubber | Establish the operating limit for the average liquid flow rate to the scrubber during the PM and HCl performance test(s) | Data from the liquid flow rate measurement device during the PSH operation stack performance test | The continuous scrubbing liquid flow rate measuring device must be accurate within plus or minus 1 percent; you must collect the flow rate data during the period of the performance test and determine the operating limit according to § 63.7112(j).
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| 16. Each FF that controls emissions from only an individual, enclosed, new or existing storage bin | Conduct opacity observations | Method 9 in appendix A-4 to 40 CFR part 60 | The test duration must be for at least 1 hour and you must obtain ten 6-minute averages.
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| 17. Fugitive emissions from any PSH operation subject to an opacity limit | Conduct opacity observations | Method 9 in appendix A-4 to 40 CFR part 60 | The test duration must be for at least 3 hours, but the 3-hour test may be reduced to 1 hour if, during the first 1-hour period, there are no individual readings greater than 10 percent opacity and there are no more than three readings of 10 percent during the first 1-hour period.
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| 18. Each building enclosing any PSH operation, that is subject to a VE limit | Conduct VE check | The specifications in § 63.7112(k) | The performance test must be conducted while all affected PSH operations within the building are operating; the performance test for each affected building must be at least 75 minutes, with each side of the building and roof being observed for at least 15 minutes.
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| 19. Each lime kiln | Measure hydrogen chloride | Method 320 or 321 of appendix A to this part or ASTM 6348-12 (Reapproved 2020)
1
2 | The test duration must be at least one hour. HCl must be used for the analyte spiking. For a positive pressure FF or ESP, determine the number of sampling points per the stratification check procedures of section 8.1.2 of Method 7E in appendix A-4 to 40 CFR part 60 using the sample points determined using the procedures of Section 8 of EPA Method 5D.
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| 20. Each lime kiln | Measure mercury | Method 29 or 30B of appendix A-8 to 40 CFR part 60 or ASTM D6784-16
2 | For Method 29 and ASTM D6784-16
2 the test duration must be at least two hours and the sample volume must be at least 1.70 dscm (60 dscf). For Method 30B, the test duration must be at least one hour and the sample volume at least 100 liters. For a positive pressure FF or ESP, use the procedures of Section 8 of EPA Method 5D for sampling points.
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| 21. Each lime kiln | Measure total organic HAP
3 | Method 18 and/or 320 in appendix A to 40 CFR part 60 and/or ASTM D6348-12 (Reapproved 2020)
1 | The test duration must be at least 1 hour. For EPA Method 320 and ASTM D6348-12 (Reapproved 2020), for a positive pressure FF or ESP, determine the number of sampling points per the stratification check procedures of section 8.1.2 of Method 7E using the sample points determined using the procedures of Section 8 of EPA Method 5D.
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| 22. Each lime kiln | Measure dioxins/furans | Method 23 in appendix A-7 to 40 CFR part 60 | The test duration must be at least 3 hours and the must be at least 3 dscm (106 dscf). For a positive pressure FF or ESP, use the procedures of Section 8 of EPA Method 5D for sampling points.
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| 23. Each lime kiln equipped with dry sorbent injection | Establish the operating limit for the dry sorbent flow rate during the HCl performance test | Data for the dry sorbent flow rate device during the HCl performance test | The flow monitor must meet the criteria in § 63.7113(h); you must collect the dry sorbent flow rate data during the period of the HCl performance test and determine the operating limit according to § 63.7112(j).
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| 24. Each lime kiln equipped with a thermal oxidizer | Establish the operating limit for the combustion chamber temperature during the total organic HAP and D/F performance test(s) | Data for the temperature device during the total organic HAP and D/F performance test(s) | The temperature device must meet the criteria in § 63.7113(i); you must collect the temperature data during the period of the total organic HAP and D/F performance test(s) and determine the operating limit according to § 63.7112(j).
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| 25. Each lime kiln equipped with activated carbon injection | Establish the operating limit for the combustion chamber temperature during the total organic HAP, D/F, and mercury performance test(s) | Data for the activated carbon flow rate device during the total organic HAP, D/F, and mercury performance test(s) | The flow monitor must meet the criteria in § 63.7113(h); you must collect the activated carbon flow rate data during the period of the total organic HAP, D/F, and mercury performance test(s)and determine the operating limit according to § 63.7112(j).
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